HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 3-(t-Butoxycarbonylamino)-2-methoxypropyl Triisopropylsilyl Ether
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 3-(t-Butoxycarbonylamino)-2-hydroxypropyl Triisopropylsilyl Ether | HCID 57936606 | — |
| Product | 3-(t-Butoxycarbonylamino)-2-methoxypropyl Triisopropylsilyl Ether | HCID 57936564 | 62% |
Reaction Steps
Using a procedure analogous to Example 57-B, 3-(t-butoxycarbonylamino)-2-hydroxypropyl triisopropylsilyl ether and methyl iodide gave the title compound (13 g, 62%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07615568B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-d4197aed26de4ca885f5552edc3b8199 |
| Source note | uspto-grants-2009_11 |