HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-2-methylthiopyrimidine → HCID 57936139, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-2-methylthiopyrimidine | HCID 97113 | — |
| Reactant | 1-(Triisopropylsilyl)pyrrole-3-boronic acid | HCID 2763303 | — |
| Product | HCID 57936139 | HCID 57936139 | 95% |
Reaction Steps
The title compound was prepared analogous to Step A of Method B, starting from [1-[tris(1-methylethyl)silyl]-1H-pyrrol-3-yl]-boronic acid and 4-chloro-2-methylsulfanyl-pyrimidine. Under the reaction conditions, the triisopropylsilyl protecting group was cleaved. Yield: 95%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07615562B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-50ae74be66bf46e9a45473fcec975560 |
| Source note | uspto-grants-2009_11 |