HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium methanethiolate → HCID 11774436, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium methanethiolate | HCID 4378561 | — |
| Reactant | HCID 11191206 | HCID 11191206 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 11774436 | HCID 11774436 | — |
Reaction Steps
Crude compound of Step B (1.4 g, 2.8 mmol) was dissolved in 10 ml MeOH and 0.4 g (5.6 mmol) sodiumthiomethylate were added. This mixture was refluxed for 7 hours. After evaporation the title compound was purified by chromatography on silicagel (DCM/MeOH/ammonia:9/1/0.1). Yield: 0.82 g (68%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07615562B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-bf5f711e568b4e64adcb39d4bec98979 |
| Source note | uspto-grants-2009_11 |