HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1434970Generated: November 3, 2026
HCID 57936114, compound → HCID 136119650, compound
https://huagongshe.com/reaction/1434970
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 57936114 | HCID 57936114 | — |
| Solvent | Hydrogen Bromide | HCID 260 | — |
| Product | HCID 136119650 | HCID 136119650 | — |
Reaction Steps
Compound of Example 152 (200 mg, 0.5 mmol) was dissolved in 10 ml hydrobromic acid 48% and stirred at 120° C. for 20 hours. Afterwards the mixture was evaporated and the crude was purified by chromatography on silicagel (DCM/MeOH/ammonia:8/2/0.2). Yield: 120 mg (62%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07615562B2 |
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| Source dataset | uspto-grants-2009_11 |
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| ORD ID | ord-d574cbccf9564b8eb593d34c2e5e14ed |
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| Source note | uspto-grants-2009_11 |
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