HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Tributylstannyl)pyridine → [4-(4-Pyridin-3-yl-phenyl)-pyrimidin-2-yl]-(2,2,6,6-tetramethyl-piperidin-4-yl)-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Tributylstannyl)pyridine | HCID 3483848 | — |
| Reactant | [4-(4-Bromophenyl)-pyrimidin-2-yl]-(2,2,6,6-tetramethyl-piperidin-4-yl)-amine | HCID 57936126 | — |
| Product | [4-(4-Pyridin-3-yl-phenyl)-pyrimidin-2-yl]-(2,2,6,6-tetramethyl-piperidin-4-yl)-amine | HCID 57936150 | — |
Reaction Steps
The title compound was prepared analogous to Step D of Example 172, starting from [4-(4-bromophenyl)-pyrimidin-2-yl]-(2,2,6,6-tetramethyl-piperidin-4-yl)-amine and 3-tributylstannanyl-pyridine. Yield: 45 mg (24%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07615562B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-3bc1673fe6c449139fdc72c182e8a604 |
| Source note | uspto-grants-2009_11 |