Sodium Azide → HCID 57936344, compound

HRID 1435018Notes

Reaction equation

HRID 1435018 reaction equation
[CH3:1][CH:2](OS(C1C=CC(C)=CC=1)(=O)=O)[CH2:3][C:4]1[CH:9]=[CH:8][C:7]([C:10]2[CH:15]=[CH:14][N:13]=[C:12]([NH:16][CH:17]3[CH2:22][C:21]([CH3:24])([CH3:23])[NH:20][C:19]([CH3:26])([CH3:25])[CH2:18]3)[N:11]=2)=[CH:6][CH:5]=1.[N-:38]=[N+:39]=[N-:40].[Na+]>CN(C=O)C>[N:38]([CH:2]([CH3:1])[CH2:3][C:4]1[CH:9]=[CH:8][C:7]([C:10]2[CH:15]=[CH:14][N:13]=[C:12]([NH:16][CH:17]3[CH2:22][C:21]([CH3:23])([CH3:24])[NH:20][C:19]([CH3:25])([CH3:26])[CH2:18]3)[N:11]=2)=[CH:6][CH:5]=1)=[N+:39]=[N-:40]

Participants

4

Reactant 2

HCID 33557Sodium AzideHCID 57936113HCID 57936113, compound

Product 1

HCID 57936344HCID 57936344, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

The title compound was prepared from toluene-4-sulfonic acid 1-methyl-2-{4-[2-(2,2,6,6-tetramethyl-piperidin-4-ylamino)-pyrimidin-4-yl]-phenyl}-ethyl ester and sodium azide in DMF.

Sources & evidence

ORD record
ord-87d571d5229e40888735c34571e6f4d7
Source dataset
uspto-grants-2009_11
Patent number
US07615562B2

Reaction notes

Loading…