HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propanoic acid, 2-bromo-2-methyl-, ethyl ester → HCID 57866374, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propanoic acid, 2-bromo-2-methyl-, ethyl ester | HCID 11745 | — |
| Reactant | Allyl Mercaptan | HCID 13367 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 57866374 | HCID 57866374 | 35% |
Reaction Steps
Ethyl 2-bromoisobutyrate (40.0 g, 0.205 mole), allyl mercaptan (16.8 g, 0.0226 mole), potassium hydroxide (14.4 g, 0.226 mole), ethyl alcohol (100 g) were combined and reaction mixture was refluxed for six hours prior to quenching. Crude yield: 79.3%; Distilled yield: 35.0%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07615661B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-03b282c9275c4e23a9c3f68c94fdbdd8 |
| Source note | uspto-grants-2009_11 |