HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanethiol → HCID 15074080, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanethiol | HCID 6343 | — |
| Reactant | Propanoic acid, 2-bromo-2-methyl-, ethyl ester | HCID 11745 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15074080 | HCID 15074080 | — |
Reaction Steps
Ethyl 2-bromoisobutyrate (28.6, 0.146 mole), ethanethiol (100 g, 0.161 mole), potassium hydroxide (10.3 g, 0.161 mole), ethyl alcohol. Stirred reaction mixture for two hours at room temperature prior to quenching. Crude yield: 117%; after kugelrohr: 77.8%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07615661B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-caf3534d23a74cbf8d4df74efea50d8d |
| Source note | uspto-grants-2009_11 |