HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Propanethiol → HCID 22627680, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Propanethiol | HCID 6364 | — |
| Reactant | Propanoic acid, 2-bromo-2-methyl-, ethyl ester | HCID 11745 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22627680 | HCID 22627680 | 61.7% |
Reaction Steps
Ethyl 2-bromoisobutyrate (100 g, 0.513 mole), 2-propanethiol (42.95 g, 0.564 mole), potassium hydroxide (36.0 g, 0.564 mole), ethyl alcohol (200 g) were combined and reaction mixture was refluxed for three hours prior to quenching. Crude yield: 74.7%, distilled yield: 61.7%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07615661B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-7380a274bc4f4f809cc00ae297b67d6b |
| Source note | uspto-grants-2009_11 |