反应详情

19.8 (34.1 mmol) g Z-D-Trp-Lys(BOC)-OMe are dissolved in 220 ml methanol, 2.2 g catalyst PdC 10% added and hydrogenated at RT. The hydrogenation is finished after 1 hour at RT, the catalyst filtered off and the filtrate evaporated at 30°: white solid. HPLC: 98.1% b.a. (16.2 min).

1. customhydrogenated at RT
2. filtrationthe catalyst filtered off
3. customthe filtrate evaporated at 30°
4. custom(16.2 min)