HuagongsheHuagongshe Chemistry Print Report · For research reference only
Z-Phg-D-Trp-Lys(BOC)-OMe → HCID 57936728, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Z-Phg-D-Trp-Lys(BOC)-OMe | HCID 57936733 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57936728 | HCID 57936728 | — |
Reaction Steps
23.4 g (23.8 mmol) (Z-Phg-D-Trp-Lys(BOC)-OMe) are dissolved in 260 ml methanol, 2.6 g Pd/C 10% added and hydrogenated at RT and normal pressure. After 3 hours the catalyst is filtered off and the filtrate evaporated at 30°: white solid. HPLC 95.9% b.a. (17.6 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07615609B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-f19814df138b43eeb7f30244518c9ebc |
| Source note | uspto-grants-2009_11 |