HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 56673352, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | [1-(Methylsulfonyl)piperidin-4-yl]amine trifluoroacetate | HCID 11975076 | — |
| Reactant | HCID 21070606 | HCID 21070606 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 56673352 | HCID 56673352 | — |
Reaction Steps
Treatment of the material prepared in Example 282 with material prepared in Example 162 in ethanol containing triethylamine at reflux for one hour, gave, after chilling and filtering, [4-amino-2-(1-methanesulfonyl-piperidin-4-ylamino)-pyrimidin-5-yl]-phenyl-methanone, as a colorless solid, MP 249-250° C. MS(ES) MH+376
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07615634B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-91a99ca0f5404055a106a9d1c3d58a2b |
| Source note | uspto-grants-2009_11 |