HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 62588378, compound → HCID 86618326, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 62588378 | HCID 62588378 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 86618326 | HCID 86618326 | — |
Reaction Steps
The above 1.26 g N-(3-Hydroxymethyl-phenyl)-3-methoxy-propionamide were dissolved in 50 ml acetone, 12.60 g manganese dioxide were added and the mixture stirred at room temperature over night. The mixture was filtered and the filtrate evaporated and further purified by chromatography on silica in ethyl acetate/heptane mixtures. Yield 0.77 g of the title compound as a colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07618964B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-9e01e3f8e78246debaa441063c6b3344 |
| Source note | uspto-grants-2009_11 |