HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorobenzenesulfonyl chloride → HCID 10133173, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorobenzenesulfonyl chloride | HCID 76187 | — |
| Reactant | 4-Thiazoleacetic acid, 2-amino-, ethyl ester | HCID 104454 | — |
| Product | HCID 10133173 | HCID 10133173 | 22% |
Reaction Steps
The tide compound was prepared from ethyl 2-amino-4-thiazolylacetate and 2-chlorobenzenesulfonyl chloride according to METHOD A, giving 0.65 g (22%) of a pink solid after recrystallization from methanol: MS (Ionspray, [M+H]+) m/z 361; Anal. Calcd (found) for C13H13ClN2O4S2: C, 43.3 (43.2)%, H, 3.6 (3.5)%, N, 7.8 (7.6)%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07618961B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-237ca8a14b704446bc7cc909af22885b |
| Source note | uspto-grants-2009_11 |