HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Bromobenzenesulphonyl chloride → HCID 10158135, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Bromobenzenesulphonyl chloride | HCID 17943 | — |
| Reactant | 4-Thiazoleacetic acid, 2-amino-, ethyl ester | HCID 104454 | — |
| Product | HCID 10158135 | HCID 10158135 | — |
Reaction Steps
The title compound was prepared from ethyl 2-amino-4-thiazolylacetate and 3-bromobenzenesulfonyl chloride according to METHOD A, using a Quest 210 apparatus and at 30° C., giving 1.16 g (27%) of an off-white solid: mp 155° C.; MS (Ionspray, [M+H]+) m/z 405; Anal. Calcd (found) for C13H13BrN2O4S2: C, 38.5 (38.4)%, H, 3.2 (3.0)%, N, 6.9 (6.6)%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07618961B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-e13e4d5e02da4c0e85b7f4231eb67bbb |
| Source note | uspto-grants-2009_11 |