HuagongsheHuagongshe Chemistry Print Report · For research reference only
o-Toluenesulfonyl chloride → HCID 10268845, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | o-Toluenesulfonyl chloride | HCID 8623 | — |
| Reactant | 4-Thiazoleacetic acid, 2-amino-, ethyl ester | HCID 104454 | — |
| Product | HCID 10268845 | HCID 10268845 | — |
Reaction Steps
The title compound was prepared from ethyl 2-amino-4-thiazolylacetate and 2-methylbenzenesulfonyl chloride according to METHOD A, giving 0.22 g (32%) of a pink powder: 1H NMR (CDCl3) δ: 1.3 (3H, t), 2.5 (3H, s), 3.9 (2H, s), 4.2 (2H, q), 6.4 (1H, s), 7.8-7.2 (3H, m), 8.1 (1H, t).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07618961B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-2e8288f3734445f6876a17d881e018d2 |
| Source note | uspto-grants-2009_11 |