HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Thiazoleacetic acid, 2-amino-, ethyl ester → HCID 10112152, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Thiazoleacetic acid, 2-amino-, ethyl ester | HCID 104454 | — |
| Reactant | 2,4-Dichloro-6-methylbenzenesulfonyl chloride | HCID 2801387 | — |
| Product | HCID 10112152 | HCID 10112152 | — |
Reaction Steps
The title compound was prepared from ethyl 2-amino-4-thiazolylacetate and 2,4-dichloro-6-methylbenzenesulfonyl chloride as described in the synthetic METHOD B to give a white solid (34.6 mg) with purity >90%: LCMS (pos) m/z 409.0, 411.0; HRMS m/z 407.9753 (calc. of monoisotopic mass for C14H14Cl2N2O4S2 gives 407.9772).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07618961B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-af91216a7b364ebf8fd9f7e8c9f6fc0b |
| Source note | uspto-grants-2009_11 |