HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-2-methylbenzene-1-sulfonyl chloride → HCID 10270797, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-2-methylbenzene-1-sulfonyl chloride | HCID 41748 | — |
| Reactant | 4-Thiazoleacetic acid, 2-amino-, ethyl ester | HCID 104454 | — |
| Product | HCID 10270797 | HCID 10270797 | — |
Reaction Steps
The title compound was prepared from ethyl 2-amino-4-thiazolylacetate and 4-chloro-2-methylbenzenesulfonyl chloride as described in the synthetic METHOD B to give a white-yellow solid (9.4 mg) with purity >90%. LCMS (pos) m/z 375.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07618961B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-e4dd90270fe2456ababdbc42fc47e7ee |
| Source note | uspto-grants-2009_11 |