HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3,4-Trichlorobenzenesulfonyl chloride → HCID 10181071, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3,4-Trichlorobenzenesulfonyl chloride | HCID 36904 | — |
| Reactant | 4-Thiazoleacetic acid, 2-amino-, ethyl ester | HCID 104454 | — |
| Product | HCID 10181071 | HCID 10181071 | — |
Reaction Steps
The title compound was prepared from ethyl 2-amino-4-thiazolylacetate and 2,3,4-trichlorobenzenesulfonyl chloride as described in the synthetic METHOD B to give a white solid (51.9 mg) with purity >90%. MS (pos) m/z 429.0, 431.0, 433.0.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07618961B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-19e90494621f49bfa3583fffc94954e4 |
| Source note | uspto-grants-2009_11 |