HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 9825028, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 91276850 | HCID 91276850 | — |
| Product | HCID 9825028 | HCID 9825028 | — |
Reaction Steps
To the compound of Step 10 dissolved in a 1/1 mixture of TBF-MeOH was added 1N NaOH. After a period of 18 h at room temperature, the reaction mixture was partitioned between saturated NH4Cl and EtOAc. The organic phase was separated, dried over Na2SO4 and evaporated to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07618979B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-3689e01dc24043e28b7049e948baa302 |
| Source note | uspto-grants-2009_11 |