HRID1435896

反应详情

EQUATION

反应方程式

HRID 1435896 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of ethyl (2E)-(1-isopropenyl-6,7-dihydro-8H-pyrido[3,4-b]-pyrrolizin-8-ylidene)ethanoate (0.40 g, 1.4 mmol) in MeOH (20 mL) was added Pd(OH)2 (0.20 g). The mixture was stirred under 1 atm of H2 for 3 h. The mixture was filtered over celite and evaporated to provide the title compound.

WORKUP

后处理

  1. filtrationThe mixture was filtered over celite
  2. customevaporated