HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → 4-Azido-3-[[(1,1-dimethylethoxy)carbonyl]amino]butanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 57938929 | HCID 57938929 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 4-Azido-3-[[(1,1-dimethylethoxy)carbonyl]amino]butanoic acid | HCID 57938930 | — |
Reaction Steps
DL-4-azido-3-tert-butoxycarbonylamino-butyric acid methyl ester (450 mg, 1.74 mmol) was dissolved in THF (12 mL) and hydrolized by adding an aqueous solution of LiOH (393 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07618982B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-15ac9e3f64d24f738cddb9f1e53b4811 |
| Source note | uspto-grants-2009_11 |