HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloride methanol → Hydrochloric Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloride methanol | HCID 21893726 | — |
| Reactant | HCID 67243419 | HCID 67243419 | — |
| Product | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 67242317 | HCID 67242317 | — |
Reaction Steps
Intermediate 20 (0.157 g) prepared in Step A mentioned above is added with 10% hydrogen chloride/methanol (2 ml), and the mixture is stirred at room temperature for 12 hours. The solvent is evaporated under reduced pressure to obtain the title compound as hydrochloride (125 mg (predictive yield)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07618984B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-dc3c812f30fd41919d23750e65b4bbc1 |
| Source note | uspto-grants-2009_11 |