HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → HCID 57938786, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | (2-chloro-quinazolin-4-yl)-(6-methoxy-pyridin-3-yl)-methylamine | HCID 11558497 | — |
| Product | HCID 57938786 | HCID 57938786 | — |
Reaction Steps
The title compound was prepared from (2-chloro-quinazolin-4-yl)-(6-methoxy-pyridin-3-yl)-methyl-amine (12 mg, 0.040 mmol) and ethanolamine (28 μl) by a procedure similar to example 10 and was isolated as off white solid (8 mg, 66%). 1H NMR (CDCl3): 8.03 (brd, J=3.0 Hz, 1H), 7.47-7.35 (m, 3H), 6.91 (brd, J=8.7 Hz, 1H), 6.78-6.73 (m, 2H), 5.56 (brs, 1H), 3.94 (s, 3H), 3.93-3.90 (m, 2H), 3.70-3.56 (m, 2H), 3.48 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07618975B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-95e53b40e7b74f54b1d65e686bdf1213 |
| Source note | uspto-grants-2009_11 |