HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → HCID 14088361, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | Methyl 2-chloropropionate | HCID 28659 | — |
| Product | HCID 14088361 | HCID 14088361 | 91.5% |
Reaction Steps
Ethanolamine (13.45 g, 0.22 mol) is added to 21.5 ml (0.2 mol) of 2-chloropropionic acid methylester. The mixture solidifies after standing at room temperature for 60 h. The solid is triturated with ethylacetate, the crystals are filtered off and dried to afford 27.75 g of the title compound as white crystals, mp. 64° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07619050B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-90585022ac264aae91cafcc4fef8a412 |
| Source note | uspto-grants-2009_11 |