Triethylamine → HCID 57939117, compound

Participants

Reaction Steps

In analogy to Example 3C) are reacted 8.43 g (0.0205 mol) (1-{tert-butyl-[1-(2-hydroxy-ethylcarbamoyl)-ethoxy]-amino}-2,2-dimethyl-propyl)-phosphonic acid diethyl ester, 2.08 g (0.025 mol) acryloylchloride and 3.2 ml (0.025 mol) triethylamine to afford the title compound as two diastereomers: 4.79 g of a colorless oil and 3.5 g of a white solid, mp 95-98° C.

Provenance & Evidence