Diethanolamine → HCID 60949092, compound

HRID 1436358Notes

Reaction equation

HRID 1436358 reaction equation
[NH:1]([CH2:5][CH2:6][OH:7])[CH2:2][CH2:3][OH:4].C[O:9][C:10](=O)[CH:11]([Cl:13])[CH3:12]>>[Cl:13][CH:11]([CH3:12])[C:10]([N:1]([CH2:5][CH2:6][OH:7])[CH2:2][CH2:3][OH:4])=[O:9]

Participants

3

Reactant 2

HCID 8113DiethanolamineHCID 28659Methyl 2-chloropropionate

Product 1

HCID 60949092HCID 60949092, compound

Procedure

Diethanolamine (10.51 g, 0.1 mol) is added to 12.25 (0.1 mol) of 2-chloropropionic acid methylester. The mixture is stirred for 24 h at room temperature. The formed methanol is evaporated to afford 18.8 g of the title compound as slightly yellow oil.

Workup

  1. customThe formed methanol is evaporated

Sources & evidence

ORD record
ord-2048c9420e6a4fd789317cdf4f84b5b5
Source dataset
uspto-grants-2009_11
Patent number
US07619050B2

Reaction notes

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