HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → 2-(2-Methyl-3-nitrophenyl)acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | (2-Methyl-3-nitrophenyl)acetonitrile | HCID 13530896 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2-(2-Methyl-3-nitrophenyl)acetic acid | HCID 13530897 | — |
Reaction Steps
150 g of 2-Methyl-3-nitro phenylacetonitrile is added to 750 ml pure water and 600 ml acetic acid. 675 ml sulfuric acid is added drop wise to the reaction mixture and refluxed for 6-7 hours. After completion of reaction, 2000 ml water is added to it and stirred for 30-45 minutes, filtered and dried to give 2-Methyl-3-nitro phenylaceticacid (130-135 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07619095B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-1365eab2af8141cd99c4161881de6fb0 |
| Source note | uspto-grants-2009_11 |