HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Phenylpiperazine → HCID 135471272, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Phenylpiperazine | HCID 250673 | — |
| Reactant | 8-chloro-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one | HCID 3653116 | — |
| Product | HCID 135471272 | HCID 135471272 | 69.4% |
Reaction Steps
8-Chloro-5,10-dihydro-dibenzo[b,e][1,4]diazepine-11-one (25 mg, 0.1 mmol) and 2-phenylpiperazine (162 mg, 1.0 mmol) were reacted according to GP4 to give 27 mg of the title compound (160FE45). MS (ESI) 389 (MH+). Purity for MH+ (UV/MS) 100/89.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07622461B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-420e8517e58e4bc785e267fc6c3472c7 |
| Source note | uspto-grants-2009_11 |