Malonic Acid → HCID 178443390, compound

Participants

Reaction Steps

3.0 g (7.5 mmol) of the compound (1) of Working Example 38 was dissolved in 30 ml of 70% aqueous acetonitrile, and to the solution was added 0.85 g (8.17 mmol) of malonic acid. The mixture was dissolved by heating, and then cooled to obtain 3.0 g of colorless crystals having a melting point of 109 to 112° C.

Provenance & Evidence