HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68893738, compound → HCID 10152043, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68893738 | HCID 68893738 | — |
| Reactant | HCID 68896318 | HCID 68896318 | — |
| Product | HCID 10152043 | HCID 10152043 | 11.8% |
Reaction Steps
This compound was prepared following the procedure described in example 4, parts E and F, starting with 1.5 g (5.3 mmol) of 1-furan-3-ylmethyl-3-piperidin-4-yl-1H-pyrrolo[2,3-b]pyridine and 1.7 g (6.9 mmol) of 2-(2-chloroethoxy)-4-chlorobenzoic acid methyl ester. After standard work-up and purification, 0.3 g (10% yield) of 4-chloro-2-{2-[4-(1-furan-3-ylmethyl-1H-pyrrolo[2,3-b]pyridin-3-yl)-piperidin-1-yl]-ethoxy}-benzoic acid were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07622480B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-5a7e30b189f04fa1a0126e7e9a367615 |
| Source note | uspto-grants-2009_11 |