HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromoethyl ethyl ether → HCID 68895392, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromoethyl ethyl ether | HCID 61141 | — |
| Reactant | HCID 68895624 | HCID 68895624 | — |
| Product | HCID 68895392 | HCID 68895392 | 63% |
Reaction Steps
This compound was prepared following the procedure described in example 24, part C, starting with 1.05 g (3.84 mmol) of 4-(1H-pyrrolo[2,3-c]pyridin-3-yl)-piperidine-1-carboxylic acid ethyl ester and 0.52 ml (4.61 mmol) of 2-bromoethylethyl ether. After standard work-up and purification, 0.83 g (63% yield) 4-[1-(2-ethoxyethyl)-1H-pyrrolo[2,3-c]pyridin-3-yl]-piperidine-1-carboxylic acid ethyl ester were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07622480B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-7cda3d56aef54757a08fd83dd7fc5e73 |
| Source note | uspto-grants-2009_11 |