HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2-(2-chloroethoxy)benzoate → HCID 68896923, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2-(2-chloroethoxy)benzoate | HCID 9837283 | — |
| Reactant | HCID 68895650 | HCID 68895650 | — |
| Product | HCID 68896923 | HCID 68896923 | 52.1% |
Reaction Steps
This compound was prepared following the procedure described in example 4, part E, starting with 0.46 g (1.7 mmol) of 1-(2-ethoxyethyl)-3-piperidin yl-1H-pyrrolo[2,3-c]pyridine and 0.44 g (2.0 mmol) of 2-(2-chloroethoxy)-benzoic acid methyl ester. After standard work-up and purification, 0.2 g (21% yield) of 2-(2-{4-[1-(2-ethoxyethyl)-1H-pyrrolo[2,3-c]pyridin-3-yl]-piperidin-1-yl}-ethoxy)benzoic acid methyl ester were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07622480B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-342ed4ba81694ddc8affc5486e48fb12 |
| Source note | uspto-grants-2009_11 |