HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine, hydrochloride → N,N-Dimethylpiperidine-2-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine, hydrochloride | HCID 10473 | — |
| Reactant | N-benzyloxypiperidine-2-carboxylic acid | HCID 23090179 | — |
| Product | N,N-Dimethylpiperidine-2-carboxamide | HCID 14810940 | — |
Reaction Steps
The general procedure of Referential Example 131 was repeated through use of N-benzyloxypiperidine-2-carboxylic acid (6.4 g) and dimethylamine hydrochloride (2 g), to thereby give the title compound as an oily product (3.8 g, quantitative amount).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07622471B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-53dcf794ab7046f6b03534758244f112 |
| Source note | uspto-grants-2009_11 |