HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 91006379, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 68704256 | HCID 68704256 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 91006379 | HCID 91006379 | 32% |
Reaction Steps
This was prepared from carbamate (b) (105 mg) by the procedure of Example (1m) with the exception that the crude material was subjected to chromatography on silica eluting with a 0-30% methanol in ethyl acetate gradient affording an oil (25 mg, 32%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07622481B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-af30a5ca8de542aa9d1ed865185bcc89 |
| Source note | uspto-grants-2009_11 |