HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 68701081, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 68700280 | HCID 68700280 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 68701081 | HCID 68701081 | 59.7% |
Reaction Steps
The carboxylic acid (c) (8.4 g) in DMF (100 ml) was treated with potassium carbonate (7.6 g) and iodomethane (2.8 ml) and stirred for 3 days. After evaporation of solvent, water (200 ml) was added and the solid filtered off and dried under vacuum to give the product (5.32 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07622481B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-1c3d32bde913485d9051e61f0e19c5ec |
| Source note | uspto-grants-2009_11 |