HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59427333, compound → 1,4-Dihydro-1,6-naphthyridin-4-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59427333 | HCID 59427333 | — |
| Solvent | 1,1'-Biphenyl, mixt. with 1,1'-oxybis(benzene) | HCID 24670 | — |
| Product | 1,4-Dihydro-1,6-naphthyridin-4-one | HCID 4089055 | — |
Reaction Steps
Dowtherm A (60 mL) was brought to reflux and (a) (6.3 g, 25.4 mmol) was added portionwise over 2 minutes. The mixture was heated for a further 5 minutes then allowed to cool to room temperature. The resulting solid was washed with a small amount of cold ethanol and dried in vacuo (2.6 g, 69%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07622481B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-81d8a24edc5b4869bbb01293061ff3ff |
| Source note | uspto-grants-2009_11 |