HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 24991587, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 66906071 | HCID 66906071 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 24991587 | HCID 24991587 | — |
Reaction Steps
This ester was prepared using the procedure described in Example 5, except 2-(2-chlorophenyl)-3-hydroxypropanenitrile was used in place of 2-(2-chloro-5-(difluoromethoxy)phenyl)-3-hydroxypropanenitrile. The preparation of 2-(2-chlorophenyl)-3-hydroxypropanenitrile is described in Example 13. The recovered ester product was a colorless oil (70% yield), Rf 0.3 (silica gel, ethyl acetate:hexane=1:4).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07622504B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-362a429a95b04d0eba0fcf6307fe57b3 |
| Source note | uspto-grants-2009_11 |