Hydrochloric Acid → HCID 131727786, compound

HRID 1438109Notes

Reaction equation

HRID 1438109 reaction equation
[CH:1]([S:4]([C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[C@H:13]1[C@@H:17]([C:18]([O:20][CH3:21])=[O:19])[CH2:16][CH2:15][N:14]1C(OC(C)(C)C)=O)(=[O:6])=[O:5])([CH3:3])[CH3:2].[ClH:29]>>[ClH:29].[CH:1]([S:4]([C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[C@H:13]1[C@@H:17]([C:18]([O:20][CH3:21])=[O:19])[CH2:16][CH2:15][NH:14]1)(=[O:6])=[O:5])([CH3:3])[CH3:2]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 131727784HCID 131727784, compound

Product 1

HCID 131727786HCID 131727786, compound

Procedure

To 13B (0.27 g) was added hydrogen chloride (4M in dioxane, 2 mL). The reaction was stirred for 2 h at rt. The solvent was removed to give 0.18 g of 13C.

Workup

  1. customThe solvent was removed
  2. customto give 0.18 g of 13C

Sources & evidence

ORD record
ord-c0e580f002e54771ad2c1431cdd096dc
Source dataset
uspto-grants-2009_11
Patent number
US07622585B2

Reaction notes

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