Hydrochloric Acid → HCID 68436532, compound

Participants

Reaction Steps

To platinum oxide (0.16 g) was added 19C (0.4 g, 1.0 mmol) in ethanol (20 mL) and hydrogen chloride (0.15 mL) under nitrogen. The reaction was placed under hydrogen (30 psi) and stirred at rt for 1.5 h. The catalyst was filtered over celite and washed with ethanol and methanol. The filtrate and washings were combined and the solvent was evaporated to give 0.35 g of yellow solid 19D.

Provenance & Evidence