Hydrochloric Acid → HCID 68438180, compound

Participants

Reaction Steps

20F was treated with 4.0 N HCl in dioxane for 4.0 h. After removal of solvent, 20G was obtained as a white solid. 1H NMR (400 MHz, DMSO-d6) δ ppm 7.62 (d, J=8.00 Hz, 1H) 6.6-6.9 (m, 2H) 5.1 and 5.0 (d, 1H) 3.2-3.5 (m, 3H) 3.0 (m, 1H) 2.1-2.4 (m, 2H) 1.32 (d, J=7.6 Hz, 3H) 1.22 (d, J=7.6 Hz, 3H).

Provenance & Evidence