HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Ethoxy-5-ethyl-2-fluorobenzaldehyde → 5-Ethyl-2-fluoro-3-methoxybenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Ethoxy-5-ethyl-2-fluorobenzaldehyde | HCID 57942802 | — |
| Reactant | 3-{[tert-Butyl(dimethyl)silyl]oxy}-5-ethyl-2-fluorobenzaldehyde | HCID 59838072 | — |
| Product | 5-Ethyl-2-fluoro-3-methoxybenzaldehyde | HCID 59838048 | — |
Reaction Steps
119A was prepared from 118C using a procedure similar to that used in the preparation of 118D. 1H NMR (400 MHz, CDCl3) δ ppm 1.23 (t, J=7.47 Hz, 3H) 2.64 (q, J=7.62 Hz, 2H) 3.92 (s, 3H) 7.02 (dd, J=8.13, 1.98 Hz, 1H) 7.23 (dd, J=5.27, 2.20 Hz, 1H) 10.35 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07622585B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-13ccbfa0e1c4440785fb163ac0a4f639 |
| Source note | uspto-grants-2009_11 |