HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanol → HCID 136354593, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | 52947-34-9 | HCID 3040798 | — |
| Product | HCID 136354593 | HCID 136354593 | — |
Reaction Steps
A solution of 12 g of methyl 3-hydroxy-benzo[b]thiphene-2-carboximidate (Example 1) in 300 m. of anhydrous n-butanol is heated under reflux for 4 hours and then concentrated to yield upon crystallization from ethyl acetate solution yellow crystals having an m.p. of 185° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04056526 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-1cc4a1ca335c486fbc1f5ded382b0e83 |
| Source note | uspto-grants-1977_11 |