HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22752998, compound → HCID 21546787, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22752998 | HCID 22752998 | — |
| Reactant | HCID 178504061 | HCID 178504061 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 21546787 | HCID 21546787 | — |
Reaction Steps
Analogously to Example 1, N-isopropyl-bis-(chlorocarbonyl)-amine (prepared analogously to Synthesis 1970, pages 542-543; boiling point 66-67° C/12 mm Hg) and acetone-S-methylisothio-semicarbazone hydroiodide, with addition of triethylamine, yielded 1-isopropyl-3-isopropylideneamino-4methylmercapto-tetrahydro-1,3,5-triazine-2,6-dione as a pale yellow powder of melting point 110-112° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04056527 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-45a243731ede4c6d81d7431fbf2a5373 |
| Source note | uspto-grants-1977_11 |