HCID 22752998, compound → HCID 21546787, compound

HRID 1438701Notes

Reaction equation

HRID 1438701 reaction equation
[CH:1]([N:4]([C:8](Cl)=[O:9])[C:5](Cl)=[O:6])([CH3:3])[CH3:2].I.[CH3:12][S:13][C:14](=[NH:20])[NH:15][N:16]=[C:17]([CH3:19])[CH3:18]>C(N(CC)CC)C>[CH:1]([N:4]1[C:8](=[O:9])[NH:20][CH:14]([S:13][CH3:12])[N:15]([N:16]=[C:17]([CH3:19])[CH3:18])[C:5]1=[O:6])([CH3:3])[CH3:2]

Participants

4

Reactant 2

HCID 22752998HCID 22752998, compoundHCID 178504061HCID 178504061, compound

Product 1

HCID 21546787HCID 21546787, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

Analogously to Example 1, N-isopropyl-bis-(chlorocarbonyl)-amine (prepared analogously to Synthesis 1970, pages 542-543; boiling point 66-67° C/12 mm Hg) and acetone-S-methylisothio-semicarbazone hydroiodide, with addition of triethylamine, yielded 1-isopropyl-3-isopropylideneamino-4methylmercapto-tetrahydro-1,3,5-triazine-2,6-dione as a pale yellow powder of melting point 110-112° C.

Sources & evidence

ORD record
ord-45a243731ede4c6d81d7431fbf2a5373
Source dataset
uspto-grants-1977_11
Patent number
US04056527

Reaction notes

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