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HRID1438701

反应详情

EQUATION

反应方程式

HRID 1438701 的结构方程式

REACTANTS

反应物

2
反应SMILES：CC(C)N(C(=O)Cl)C(=O)Cl
HCID22752998

未命名化合物

反应SMILES：CSC(=N)NN=C(C)C.I
HCID178504061

未命名化合物

PRODUCTS

产物

1
反应SMILES：CSC1NC(=O)N(C(C)C)C(=O)N1N=C(C)C
HCID21546787

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
反应SMILES：CCN(CC)CC
溶剂HCID8471

Triethylamine

C6H15N

PROCEDURE

实验过程

Analogously to Example 1, N-isopropyl-bis-(chlorocarbonyl)-amine (prepared analogously to Synthesis 1970, pages 542-543; boiling point 66-67° C/12 mm Hg) and acetone-S-methylisothio-semicarbazone hydroiodide, with addition of triethylamine, yielded 1-isopropyl-3-isopropylideneamino-4methylmercapto-tetrahydro-1,3,5-triazine-2,6-dione as a pale yellow powder of melting point 110-112° C.