HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21400252, compound → HCID 21400239, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21400252 | HCID 21400252 | — |
| Reactant | HCID 178504061 | HCID 178504061 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 21400239 | HCID 21400239 | — |
Reaction Steps
Analogously to Example 1, N-cyclohexyl-bis-(chloro-carbonyl)-amine (prepared analogously to Snythesis 1970, pages 542-543; boiling point 80°-82° C/0.3 mm Hg) and acetone-S-methylisothiosemicarbazone hydroiodide, with addition of triethylamine, yielded 1-cyclohexyl-3-isopropylideneamino-4-methylmercaptotetrahydro- 1,3,5-triazine-2,6-dione as a pale yellow powder of melting point 111°-112° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04056527 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-d538e8774fa84128b4cdb16fd342dc9e |
| Source note | uspto-grants-1977_11 |