HCID 21400252, compound → HCID 21400239, compound

HRID 1438702Notes

Reaction equation

HRID 1438702 reaction equation
[CH:1]1([N:7]([C:11](Cl)=[O:12])[C:8](Cl)=[O:9])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.I.[CH3:15][S:16][C:17](=[NH:23])[NH:18][N:19]=[C:20]([CH3:22])[CH3:21]>C(N(CC)CC)C>[CH:1]1([N:7]2[C:11](=[O:12])[NH:23][CH:17]([S:16][CH3:15])[N:18]([N:19]=[C:20]([CH3:22])[CH3:21])[C:8]2=[O:9])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

4

Reactant 2

HCID 21400252HCID 21400252, compoundHCID 178504061HCID 178504061, compound

Product 1

HCID 21400239HCID 21400239, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

Analogously to Example 1, N-cyclohexyl-bis-(chloro-carbonyl)-amine (prepared analogously to Snythesis 1970, pages 542-543; boiling point 80°-82° C/0.3 mm Hg) and acetone-S-methylisothiosemicarbazone hydroiodide, with addition of triethylamine, yielded 1-cyclohexyl-3-isopropylideneamino-4-methylmercaptotetrahydro- 1,3,5-triazine-2,6-dione as a pale yellow powder of melting point 111°-112° C.

Sources & evidence

ORD record
ord-d538e8774fa84128b4cdb16fd342dc9e
Source dataset
uspto-grants-1977_11
Patent number
US04056527

Reaction notes

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