HCID 21400241, compound → HCID 54309081, compound

HRID 1438703Notes

Reaction equation

HRID 1438703 reaction equation
[CH2:1]([N:8]([C:12](Cl)=[O:13])[C:9](Cl)=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.I.[CH3:16][S:17][C:18](=[NH:24])[NH:19][N:20]=[C:21]([CH3:23])[CH3:22]>C(N(CC)CC)C>[CH2:1]([N:8]1[C:12](=[O:13])[NH:24][CH:18]([S:17][CH3:16])[N:19]([N:20]=[C:21]([CH3:23])[CH3:22])[C:9]1=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

4

Reactant 2

HCID 21400241HCID 21400241, compoundHCID 178504061HCID 178504061, compound

Product 1

HCID 54309081HCID 54309081, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

Analogously to Example 1, N-benzyl-bis-(chlorocarbonyl)-amine and acetone-S-methyl-isothiosemicarbazone hydroiodide, with addition of triethylamine, yielded 1-benzyl-3-isopropylideneamino-4-methylmercapto-tetrahydro-1,3,5-triazine-2,6-dione as a pale brown powder of melting point 148°-150° C.

Sources & evidence

ORD record
ord-980c15fd7e044835a27da900c21a8b0c
Source dataset
uspto-grants-1977_11
Patent number
US04056527

Reaction notes

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