HCID 21400332, compound → HCID 53991329, compound

HRID 1438704Notes

Reaction equation

HRID 1438704 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]([C:12](Cl)=[O:13])[C:9](Cl)=[O:10])=[CH:4][CH:3]=1.I.[CH3:16][S:17][C:18](=[NH:24])[NH:19][N:20]=[C:21]([CH3:23])[CH3:22]>C(N(CC)CC)C>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[C:12](=[O:13])[NH:24][CH:18]([S:17][CH3:16])[N:19]([N:20]=[C:21]([CH3:23])[CH3:22])[C:9]2=[O:10])=[CH:4][CH:3]=1

Participants

4

Reactant 2

HCID 21400332HCID 21400332, compoundHCID 178504061HCID 178504061, compound

Product 1

HCID 53991329HCID 53991329, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

Analogously to Example 1, N-(4-chlorophenyl)-bis(chlorocarbonyl)-amine and acetone-S-methyl-isothiosemicarbazone hydroiodide with addition of triethylamine, yielded 1-(4-chlorophenyl)-3-isopropylideneamino-4-methylmercaptotetrahydro-1,3,5-triazine-2,6-dione as a colorless powder of melting point 142°-144° C.

Sources & evidence

ORD record
ord-5344c0a5dc71491a9e3bd00f09241cc0
Source dataset
uspto-grants-1977_11
Patent number
US04056527

Reaction notes

Loading…