HCID 21400337, compound → HCID 53909282, compound

HRID 1438705Notes

Reaction equation

HRID 1438705 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([N:9]([C:13](Cl)=[O:14])[C:10](Cl)=[O:11])[CH:5]=[CH:6][C:7]=1[Cl:8].I.[CH3:17][S:18][C:19](=[NH:25])[NH:20][N:21]=[C:22]([CH3:24])[CH3:23]>C(N(CC)CC)C>[Cl:1][C:2]1[CH:3]=[C:4]([N:9]2[C:13](=[O:14])[NH:25][CH:19]([S:18][CH3:17])[N:20]([N:21]=[C:22]([CH3:24])[CH3:23])[C:10]2=[O:11])[CH:5]=[CH:6][C:7]=1[Cl:8]

Participants

4

Reactant 2

HCID 21400337HCID 21400337, compoundHCID 178504061HCID 178504061, compound

Product 1

HCID 53909282HCID 53909282, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

Analogously to Example 1, N-(3,4-dichlorophenyl)-bis(chlorocarbonyl)-amine and acetone-S-methyl-isothiosemicarbazone hydroiodide, with addition of triethylamine, yielded 1-(3,4-dichlorophenyl)-3-isopropylideneamino-4-methylmercapto-tetrahydro-1,3,5-triazine-2,6-dione as a colorless powder of melting point 181°-182° C.

Sources & evidence

ORD record
ord-3c7f87e3d9524bffb044569cf05ecdd4
Source dataset
uspto-grants-1977_11
Patent number
US04056527

Reaction notes

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